Fragile intermediate identification and reactivity elucidation in electrochemical oxidative ?-C(sp3)–H functionalization of tertiary amines

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Chem. Sci., 2023, Advance ArticleDOI: 10.1039/D3SC00527E, Edge Article Open Access &nbsp This article is licensed under a Creative Commons Attribution-NonCommercial 3.0 Unported Licence.Kailun Liang, Dongmei Zhang, Yanming Su, Lijun Lu, Jun Hu, Yi-Hung Chen, Xinxing Zhang, Aiwen Lei, Hong YiAn online electrochemical mass spectrometry (MS) methodology has been developed and utilized to probe the short-lived intermediates in electrochemical oxidative ?-C(sp3)–H functionalization of tertiary amines.To cite this article before page numbers are assigned, use the DOI form of citation above.The content of this RSS Feed (c) The Royal Society of Chemistry

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